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I want to test a method out and see how it runs.
Really all you would need is a vacuum pump/hand pump with a simple filter top, some methanol, powder and distilled water. Should be able to purify and get a higher yield of pure product but less amount.
Then do a melting point test to verify the product.
Hey guys this caught my eye when I saw the title. The method you speak of is what we use to do with test pellets...right? I don't know if you'd lost a lot, maybe, but the pellets had fillers and such to hold together and that is basically what was lost. Maybe try a small amount first and see. Good luck